The result of such analysis is a kinetics model or method correctly describing experimental data under different temperature conditions. To replicate the effects of ageing on pyrotechnic substances, work has been done to establish the effects of thermal and humidity conditions 20,21,22,23,24,25,26,27,28,29. Using akts thermo kinetics software, the rate and the progress of the reactions can be predicted for the variety of temperature profiles such as. Study of thermal reactivity and kinetics of hmx and its pbx. Unzip the installation materials from the zipped file downloaded in the step above. Aktsthermokinetics software deliver corresponding input functions that were determined through differential scanning calorimetry tests of small. Using low thermal inertia adiabatic calorimetry data with aktsthermokinetics software. Process measurement manufactured products thermo kinetics. The ver y important feature of the akts thermokinetics software 4 is the possibilit y of the optimization of the baseline for all experiments collected by different heatin g rates or. Based on the bootstrap sets of estimated kinetic parameters, the prediction can be enhanced by the estimation of the prediction band pb in the form of, e. Advanced kineticsbased simulation of time to maximum rate under.
Aktsthermokinetics software can optimize temperature program in such a way that it allows to obtain the value of the reaction rate set by the user. The software allows for the analysis of temperaturedependent processes. The dsc experiments were carried out in sealed crucibles 5 from room temperature till 260c with various heating rates. We have also included a powerful search engine that will enable you to. The kinetic analysis of a heavily aluminized cyclotrimethylenetrinitramine rdx using differential scanning calorimetry dsc is conducted. May 02, 2018 akts thermokinetics software version 4. In addition, having the kinetic description of the reaction rate derived from the dsc data, one can estimate that the reaction progress. Jul 15, 2019 to replicate the effects of ageing on pyrotechnic substances, work has been done to establish the effects of thermal and humidity conditions 20,21,22,23,24,25,26,27,28,29. Aktsthermokinetics software prediction of thermal aging of materials by modified kinetic analysis based on limited amount of experimental points the investigation of materials aging at ambient temperatures is experimentally very difficult due to its very low rate, small changes of physicochemical properties and, very often, limited amount of. Click the loginregister button for further information and to download iq 20 nov 2014.
Thermal aging discontinuous data collection setaram. The most popular versions among the software users are 3. The ver y important feature of the aktsthermokinetics software 4 is the possibilit y of the optimization of the baseline for all experiments collected by different heatin g rates or. Figure 6 dsc curves for a pyrotechnic delay according to moistureinduced ageing. The application the thermal safety software and the kineticsbased approach led to proper selection of experimental conditions for sadt testing. The thermokinetics and degradation process of soybean oil. We have also included a powerful search engine that will enable you to find the most applicable data. Not sure if its within your budget but with tgdsc information, akts makes some powerful thermokinetics packages. Dependence of the activation energy of the combustion on the reaction progress evaluated with aktsthermokinetics software. Nonisothermal cold crystallization kinetics of polylactic acid. Using low thermal inertia adiabatic calorimetry data with akts. Thermal analysis and thermokinetics softwares setaram.
Using akts thermokinetics software, the rate and the progress of the reactions can be predicted for the variety of temperature profiles such as. Akts thermokinetics software and aktsthermal safety software. Kinetic parameters were calculated using aktsthermokinetics software 1 based on differential isoconversional approach 2, 3. Pharmaceutics free fulltext solid state stability and. Oct 23, 2019 dynamic calculations for combustion of the pyrotechnic delay were performed using akts thermokinetics software 10. Akts thermokinetics software deliver corresponding input functions that were determined through differential scanning calorimetry tests of small explosive samples. View the application notes in your field, available for download, by visiting a huge database is in the application library area of our website. Pentaho business intelligence suite is software developed by pentaho.
Influence of potassium chloride on the thermal decomposition of. Polyurethane pu production with the use of soybean oil was greatly appreciated by researchers due to their low cost, easy availability, and nontoxic nature. Thermal aging continuous data collection thermal aging discontinuous data collection thermal safety reaction calorimetry sml calisto. Evaluating sadt by advanced kineticsbased simulation approach. Using aktsthermokinetics software, the rate and the progress of the reactions can be predicted for the variety of temperature profiles such as. Pdf extended multiphysics model for slowcook off events. Synergy in cocombustion of oil shale semicoke with. The simulations presented in this study were done with the aktsthermokinetics software. Netzsch kinetics neo software is used to analyze chemical processes. This download was checked by our builtin antivirus and was rated as safe. Dependence of the activation energy of the combustion on the reaction progress evaluated with akts thermokinetics software. Akts offer thermogravimetry, thermal analysis and solid state kinetic analysis of ms and ftir data. Applications specifications45 c to 120 c cooling under 0 c requires the use.
Vacuum stability test vst was used to determine the thermal behavior and kinetic parameters of 1, 3, 5, 7tetranitro1, 3, 5, 7tetrazocine hmx and its mixture with hydroxylterminated polybutadiene htpb as a binder coded as hmxhtpb. Aktsthermokinetics software setaram instrumentation. Model fitting and isoconversional method were applied to determine the kinetic parameters based on vst results. The program lies within education tools, more precisely science tools. With akts thermokinetics software 32 it can be demonstrated that a two steps model combination with zeroth and second order kinetics is recommended for accurate simulations. Thermal aging continuous data collection setaram inc. Everything has been done to simplify your temperature controls. This period is measured from the time when the temperature in the center of the. Analysis and specific safety concepts produced for customers by akts thermal safety software are optimized for costeffectiveness and apply stateoftheart technology. Fast sybr green master mix on biorad cfx96, biorad iq5, and lc 480. Thermal aging discontinuous data collection download viewer. Kinetics download on macbook in english aprausunkibe92s blog. Thermokinetics deals with the study of thermal decomposition kinetics see also. After application of the heat balance to compare the amount of heat generated.
Processing, design, quality control, and operational applications all require. Akts thermokinetics software background critical process safety and thermal stability parameters tmrad, sadt, etc. Aktsthermokinetics software enables advanced baseline construction ten 10 different baseline types tangential sigmoid, tangential first point, tangential last point, sigmoid, spline, straight, horizontal last point, equal to zero baseline, staged because the correct baseline selection is one of the most critical parts of data treatment. The main goal of aktsthermokinetics software package is to facilitate kinetic analysis of. Is there any open access software that can be used to calculate. Combine our software platforms with our extensive and searchable spectral libraries for easier. Akts thermokinetics software and aktsthermal safety software, com. The tenfold increase of the mass from 550 kg results in the decrease of the sadt from 50 to 43c.
Dha laboratory products fauske and associates, llc. Advanced thermokinetics software for kinetic analysis and thermal safety a global solution for kinetic analysis and determination of the thermal stability of materials setaram instrumentation and akts software have formed a partnership to provide a global solution for kinetic analysis and determination of the thermal stability of materials the akts software can be. Id 47 mm, length 200 mm, wall thickness 4 mm and the volume of. Mass spectrometry software thermo fisher scientific us. Combined with the extensive knowledge and experience of our team, and complemented by the products of our principals, we can help you find. Only users with a maintenance period after december 19th, 2019 can upgrade to akts thermokinetics 5. The cookoff experiments were carried out in cylindrical steel tube with. Dynamic calculations for combustion of the pyrotechnic delay were performed using aktsthermokinetics software 10.
Application of vacuum stability test to determine thermal. Determination of the kinetic characteristics step 2 4. Akts advanced thermal analysis software dsc dta tg tgms tg. Use the included memory card to store your ambient, infrared, and probe temperatures in an excelcsv file or download the free software and connect the ir75pro to your pc with the included usb cable for real time monitoring and data capture. The tenfold increase of the mass from 5 to 50 kg results in the decrease of the sadt from 50 to 43 c. The friedman isoconversional method is applied to dsc experimental data and akts software is used for the analysis. A brief tour of akts software discover the outstanding possibilities of the four software packages and download a demonstration. Akts software is a global solution for kinetic analysis and determination of the thermal stability of materials. Due to their precise determination, the variation of the runaway time under true adiabatic mode.
The software can analyze different types of thermal curves depicting the changes to a given. Critical process safety and thermal stability parameters tmrad, sadt, etc. Sadt is defined as the lowest environmental temperature at which the center of the material within the package heats to a temperature 6 c greater than the environmental temperature after a lapse of a seven day period or less. The results of dsc experiments carried out with different heating rates in the range of 0.
The actual developer of the software is thermodata. It is often the case in industrial applications, that in order to achieve a certain characteristic profile, high quality or specific sample properties, thermal reaction rates should be very. A graph in 2 clicks and all information to decide at a glance. In the akts thermokinetics software, go to the menu administration automatic upgrade. Power sybr green master mix on biorad cfx96, biorad iq5, and lc 480. The preexponential factor and activation energy are extracted as a function of product mass fraction. Use of the model allows for predictions of a chemical systems. Natas 2011 consideration of autocatalytic behavior in determination of self accelerating decomposition temperature what is a self. Using low thermal inertia adiabatic calorimetry data with akts thermokinetics software. Analysis and specific safety concepts produced for customers by akts thermal safety software are. Analysis and specific safety concepts produced for customers by aktsthermal safety software are. Determination of the reaction kinetics, describing the rate of heat generation, and the heat balance in the system, based on frankkamenetskii approach, was calculated using akts thermokinetics and thermal safety software.
Click the download button to download the installer to your computer. Akts thermokinetics software prediction of thermal aging of materials by modified kinetic analysis based on limited amount of experimental points the investigation of materials aging at ambient temperatures is experimentally very difficult due to its very low rate, small changes of physicochemical properties and, very often, limited amount of. Manufactured products innovative, valuedriven process measurement products for industry. Study of thermal reactivity and kinetics of hmx and its.
A noncalorimetric approach for investigating the moisture. Thermokinetics study of degradation process of soybean. Aktsthermokinetics software prediction of shelf life of. The complete pc software to program and read your thermo buttons, hygro buttons and ibtags. Akts advanced kinetic and technology solution program 21 requires input of different heating rates.
If the computer where akts thermokinetics is installed is connected to internet online. Download and read fracture kinetics of crack growth fracture kinetics of crack growth interestingly, fracture kinetics of crack growth that you really wait for now is. Calculations with the akts software increase the accuracy of the estimated kinetic parameters. Providing our customers with comprehensive solutions for diverse applications coupled with the added value of expert assistance, quality products and time sensitivity, while maintaining our high standards and attention to detail. Akts thermokinetics software for comprehensive investigation of reaction or decomposition. When reading a thermo or hygro button, the graph is automatically displayed, as well as the list of values. This software utilizes an advanced differential isoconversional kinetic techniques for the precise modeling of runaway chemical reactions.
Kinetics download on macbook in english aprausunkibe92s. View the application notes in your field, available for. Thermo kinetics manufactures a comprehensive line of products for temperature and process measurement and control. Akts advanced thermal analysis software dsc dta tg tgms. In akts thermokinetics software we propose the modification of the kinetic analysis which allows the. Isoconversional method for extracting reaction kinetics of. In this case you are visiting the service center to retrieve the the latest version installation, so thats shown first. Simplify your ms and msms analyses with our mass spectrometry software platforms, which feature intuitive and userfriendly interfaces that easily acquire, analyze, manage, and report data generated by lcms, gcms, irms, and icpms systems.
Analysis and specific safety concepts produced for customers by aktsthermal safety software are optimized for costeffectiveness and apply stateoftheart technology. Aktsthermokinetics akts advanced thermal analysis software. Akts thermokinetics software thermal aging version discontinuous data collection the main goal of akts thermokinetics software package is to facilitate kinetic analysis of dsc, dta, tga, ega tgms, tgftir data for the study of the thermal behaviour of raw materials and products within the scope of research, development and quality assurance. Determination of thermal hazard from dsc measurements. Whats new in aktsthermokinetics akts advanced thermal. The prediction bands, marked by the dashed lines, were determined by the bootstrap method see text. Towards understanding the effects of heat and humidity on. An advanced solution for thermal stability determination and safety analysis introduction generally, all energetic materials evolve heat during decomposition. Includes downloads, online sample submission and contacts in siders, switzerland. Thermo kinetics software package is to facilitate kinetic analysis of dsc, dta, and tg data for the study of the thermal behavior of materials within. Thermal aging continuous data collection download viewer. Thermo kinetics software package is to facilitate kinetic analysis of dsc, dta, and tg data for the study of the thermal behavior of materials within the scope of research and development.
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